Valerii P. Sazonov 0 -2e+00 Ambient temperature 1 -2 °C 2 2.71e+02 Ambient temperature 3 2.71 $\pu{K}$ Ambient temperature °C 75-76.5 1 1 Solubility, Solubility data series The synthetic method was used. Miscibility was determined in a glass-stoppered tube of 4 mm inside diameter. Equal volumes (0.1 mL) of (1) and (2) were measured into the tube which was then strapped to a thermometer, warmed to 5 or 10 °C above the solubility temperature, mixed well by shaking, and then allowed to cool slowly, still shaking, in a bath of white oil, water or (below 0 °C) non-freezing mixture. The International Union of Pure and Applied Chemistry Mulliken, S. P.; Wakeman, R. L.; Recl. Trav. Chim. Pays-Bas, 54, 366-72 (1935). paper https://doi.org/10.1002/recl.19350540508 75-52-5 1 CH3NO2 InChI=1S/CH3NO2/c1-2(3)4/h1H3 LYGJENNIWJXYER-UHFFFAOYSA-N 61.04 Nitromethane Not specified. 926-56-7 2 C6H10 InChI=1S/C6H10/c1-4-5-6(2)3/h4-5H,1H2,2-3H3 CJSBUWDGPXGFGA-UHFFFAOYSA-N 82.14 4-Methyl-1,3-pentadiene Some alkadienes(*) were obtained from Dr. F. Cortese; others were purest commercial samples available from BDH. Nitromethane with 4-Methyl-1,3-pentadiene