Marie C. Haulait-Pirson Solubility, Solubility data series A method of gravimetric absorption monitored by tritium tracer was used. (1) was equilibrated with a slight excess of titrated water by shaking over a period of at least 8 hr in a thermostat. The phases were allowed to separate for at least 16 hr and then were sampled for tritium analysis. Most of the (1) phase was weighed into a boiling flask of a closed distillation system and then distilled through a magnesium perchlorate weighing tube. The magnesium perchlorate was then dissolved for measurement of its tritium content by liquid scintillation counting with a Packard Tri-Carb Scintillation Spectrometer. The International Union of Pure and Applied Chemistry Goldman, S.; Can. J. Chem. 1974, 52, 1668-80. paper https://doi.org/10.1139/v74-241 Roddy, J. W.; Coleman, C. F.; Talanta 1968, 15, 1281-6. paper https://doi.org/10.1016/0039-9140(68)80050-5 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water tritiated water at 5 Ci/mL; New England Nuclear Corp.; diluted to about 1 mCi/mL. 110-82-7 1 C6H12 InChI=1S/C6H12/c1-2-4-6-5-3-1/h1-6H2 XDTMQSROBMDMFD-UHFFFAOYSA-N 84.1595 Cyclohexane source not specified; spectralgrade reagent. Cyclohexane with Water