Andrzej Maczynski, Z. Maczynska, A. Szafranski Solubility, Solubility data series In a serum cap-sealed 4-oz. Brown glass bottle immersed in a water bath, (1) was saturated with (2) at 20 ± 0.02 °C for seven days. A 20-mL sample was withdrawn with a silicone-hydrophobized hypodermic syringe pushed about 2/3 of the way into the hydrocarbon liquid. Stabilized Karl Fischer reagent diluted to a titer of 1.0-1.3 mg(2)/mL was used to titrate (2) in (1) directly in the presence of methanol to a dead-stop end-point using a Beckman KF3 automatic titrimeter with a 5-mL miroburet. The International Union of Pure and Applied Chemistry Schatzberg, P.; J. Phys. Chem. 1963, 67, 776-9. paper https://doi.org/10.1021/j100798a014 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Distilled and deionized. 71-43-2 1 C6H6 InChI=1S/C6H6/c1-2-4-6-5-3-1/h1-6H UHOVQNZJYSORNB-UHFFFAOYSA-N 78.1118 Benzene Matheson, Coleman and Bell Chromatoquality reagent 99+ mole%; used as received. Benzene with Water