Andrzej Maczynski, Z. Maczynska, A. Szafranski 1 2.5e+01 Ambient temperature 2 2.5 °C -4 5.7e-04 Solubility (v/v) (2 in 1) 2 5.7 $\pu{cm3(\rm{2})/cm3(\rm{1})}$ 1 1 3.0e+01 Ambient temperature 2 3.0 °C -4 6.5e-04 Solubility (v/v) (2 in 1) 2 6.5 $\pu{cm3(\rm{2})/cm3(\rm{1})}$ 2 1 3.5e+01 Ambient temperature 2 3.5 °C -4 7.5e-04 Solubility (v/v) (2 in 1) 2 7.5 $\pu{cm3(\rm{2})/cm3(\rm{1})}$ 3 1 Solubility, Solubility data series In a thermostatted glass stoppered flask 10-25 mL (1) was shaken for min four hours. with tritiated water (a few mL of $\ce{HTO}$ equivalent to ca. 2 mCi/mL) and decanted. A 5-mL aliquot was re-shaken for four hours. with 5 mL $\ce{H2O}$ in a 10 mL flask, sampled and assayed with a Nuclear Enterprises type 8301 liquid scintillation counter. The two-stage process eliminates quenching effects (due to solvent) on the scintillator. The International Union of Pure and Applied Chemistry Vogel 'Practical Organic Chemistry' Longmans, Green and Co., London, 1956. book Jones, J. R.; Monk, C. B.; J. Chem. Soc. 1963, 2633-5. paper https://doi.org/10.1039/jr9630002633 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Not specified. 71-43-2 1 C6H6 InChI=1S/C6H6/c1-2-4-6-5-3-1/h1-6H UHOVQNZJYSORNB-UHFFFAOYSA-N 78.1118 Benzene "Analar" grade; repurified by conventional methods [1]. Benzene with Water