W.Y. Shiu, D. Mackay Solubility, Solubility data series A saturated solution of (1) was prepared by pumping salt water through a 'generation column' which was packed with glass beads coated with 1% by weight of (1). The saturated solution was extracted with an 'extractor column' packed with a superficially porous bonded $\ce{C18}$ stationary phase, then a wateracetonitrile solvent was passed through for extraction. The extract was introduced into a liquid chromatograph and the concentration of (1) was measured with a UV detector. The International Union of Pure and Applied Chemistry May, W. E.; Wasik, S. P.; Freeman, D. H.; Anal. Chem. 1978, 50, 997-1000 paper https://doi.org/10.1021/ac50029a042 7647-14-5 2 NaCl InChI=1S/ClH.Na/h1H;/q;+1/p-1 FAPWRFPIFSIZLT-UHFFFAOYSA-M 58.443 Sodium chloride reagent grade. 7732-18-5 3 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water distilled from potassium-sodium hydroxide and passed through an XAD-2 column. 71-43-2 1 C6H6 InChI=1S/C6H6/c1-2-4-6-5-3-1/h1-6H UHOVQNZJYSORNB-UHFFFAOYSA-N 78.1118 Benzene Greater than 97% pure. Benzene with Sodium Chloride and Water