Marie C. Haulait-Pirson 1 2.5e+01 Ambient temperature 2 2.5 °C -4 6.1e-04 Mole fraction - Liquid (2) 2 6.1 1 1 6e+01 Relative mass - solution (2) 1 6 mg/kg 1 1 4.0e+01 Ambient temperature 2 4.0 °C -3 1.26e-03 Mole fraction - Liquid (2) 3 1.26 1 2 1.23e+02 Relative mass - solution (2) 3 1.23 mg/kg 2 1 Solubility, Solubility data series (1) was saturated by storing over a layer of (2) in a brown glass bottle without any agitation. The bottle was sealed with serum cap and completely submerged in the water-bath for seven days. A 20-mL sample was withdrawn with a silicone-hydrophobized hypodermic syringe. Stabilized Karl Fischer reagent diluted to a titer of 1.0-1.3 mg (2)/mL was used to titrate (2) in (1) directly in the presence of methanol to a 'dead-stop' end-point using a Beckman KF3 automatic titrimeter. The International Union of Pure and Applied Chemistry Schatzberg, P.; J. Phys. Chem. 1963, 67, 776-9. paper https://doi.org/10.1021/j100798a014 629-50-5 1 C13H28 InChI=1S/C13H28/c1-3-5-7-9-11-13-12-10-8-6-4-2/h3-13H2,1-2H3 IIYFAKIEWZDVMP-UHFFFAOYSA-N 184.361 Tridecane Phillips Petroleum Co.; research grade; 99.73 mole%; passed repeatedly through a column of silica gel until no absorption occurred in the 220 to 340 nm spectral range. 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Distilled and deionized. Tridecane with Water