Andrzej Maczynski, Z. Maczynska Solubility, Solubility data series A mixture of (1) and (2) was rotated for twenty hours in a constant temperature bath at 25 °C. A sample (5 - 20 mL) of the aqueous phase was withdrawn and extracted with a measured volume of hexane (10 - 50 mL) by shaking in a glass-stoppered Erlenmeyer flask. Next, the absorbance of the hexane phase was measured against a hexane blank on the Beckman spectrophotometer. The International Union of Pure and Applied Chemistry Andrews, L. J.; Keefer, R. M.; J. Am. Chem. Soc. 1949, 71, 3644-77. paper https://doi.org/10.1021/ja01179a018 85-01-8 1 C14H10 InChI=1S/C14H10/c1-3-7-13-11(5-1)9-10-12-6-2-4-8-14(12)13/h1-10H YNPNZTXNASCQKK-UHFFFAOYSA-N 178.229 Phenanthrene Eastman Kodak Co., best grade; recrystallized twice from ethanol; MP = 101.0°C. 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water not specified. Phenanthrene with Water