Valerii P. Sazonov 1 5.50e+01 Ambient temperature 3 5.50 °C 2 3.282e+02 Ambient temperature 4 3.282 $\pu{K}$ 1 1 5.65e+01 Ambient temperature 3 5.65 °C 2 3.297e+02 Ambient temperature 4 3.297 $\pu{K}$ 2 1 6.10e+01 Ambient temperature 3 6.10 °C 2 3.342e+02 Ambient temperature 4 3.342 $\pu{K}$ 3 1 6.40e+01 Ambient temperature 3 6.40 °C 2 3.372e+02 Ambient temperature 4 3.372 $\pu{K}$ 4 1 6.50e+01 Ambient temperature 3 6.50 °C 2 3.382e+02 Ambient temperature 4 3.382 $\pu{K}$ 5 1 6.80e+01 Ambient temperature 3 6.80 °C 2 3.412e+02 Ambient temperature 4 3.412 $\pu{K}$ 6 1 6.85e+01 Ambient temperature 3 6.85 °C 2 3.417e+02 Ambient temperature 4 3.417 $\pu{K}$ 7 1 7.10e+01 Ambient temperature 3 7.10 °C 2 3.442e+02 Ambient temperature 4 3.442 $\pu{K}$ 8 1 7.15e+01 Ambient temperature 3 7.15 °C 2 3.447e+02 Ambient temperature 4 3.447 $\pu{K}$ 9 1 7.35e+01 Ambient temperature 3 7.35 °C 2 3.467e+02 Ambient temperature 4 3.467 $\pu{K}$ 10 1 7.40e+01 Ambient temperature 3 7.40 °C 2 3.472e+02 Ambient temperature 4 3.472 $\pu{K}$ 11 1 7.50e+01 Ambient temperature 3 7.50 °C 2 3.482e+02 Ambient temperature 4 3.482 $\pu{K}$ 12 1 7.50e+01 Ambient temperature 3 7.50 °C 2 3.482e+02 Ambient temperature 4 3.482 $\pu{K}$ 13 1 Solubility, Solubility data series The synthetic method was used. A Reichert microscope, type RCH, equipped with a heating stage was used as described elsewhere [1]. The disappearance and reappearance of the interface between (1) and (2) could be observed without difficulty. The International Union of Pure and Applied Chemistry Schmid, H. H. O.; Mangold, H. K.; Lundberg, W. O.; J. Am. Oil Chem. Soc. 42, 372 (1965). paper https://doi.org/10.1007/bf02635572 Schmid, H. H. O.; Mangold, H. K.; Lundberg, W. O.; Microchem. J. 9, 134-144 (1965). paper https://doi.org/10.1016/0026-265x(65)90094-9 75-05-8 1 C2H3N InChI=1S/C2H3N/c1-2-3/h1H3 WEVYAHXRMPXWCK-UHFFFAOYSA-N 41.052 Acetonitrile Baker Chemical Co.; reagent No. 9011; $n_{D}^{20}$ = 1.3445, $d_{4}^{20}$ = 0.780. 111-61-5 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20(21)22-4-2/h3-19H2,1-2H3 MVLVMROFTAUDAG-UHFFFAOYSA-N 312.53 Ethyl octadecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 66455-49-0 2 C20H40O2 InChI=1S/C20H40O2/c1-2-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-22-20-21/h20H,2-19H2,1H3 HNKCZZOHAXMGMR-UHFFFAOYSA-N 312.53 Nonadecyl formate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 822-23-1 2 C20H40O2 InChI=1S/C20H40O2/c1-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-22-20(2)21/h3-19H2,1-2H3 OIZXRZCQJDXPFO-UHFFFAOYSA-N 312.53 Octadecyl acetate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 1731-94-8 2 C20H40O2 InChI=1S/C20H40O2/c1-3-4-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-20(21)22-2/h3-19H2,1-2H3 BDXAHSJUDUZLDU-UHFFFAOYSA-N 312.53 Methyl nonadecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 66455-48-9 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-6-7-8-9-10-11-12-13-14-15-16-17-18-19-22-20(21)4-2/h3-19H2,1-2H3 CHQQYYTVIJYGOS-UHFFFAOYSA-N 312.53 Heptadecyl propanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 6221-99-4 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-6-7-8-9-10-11-12-13-14-15-16-17-19-22-20(21)18-4-2/h3-19H2,1-2H3 NJVKAQGGBANCKG-UHFFFAOYSA-N 312.53 Hexadecyl butanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 26718-84-3 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-6-7-8-9-10-11-12-13-14-15-16-17-18-20(21)22-19-4-2/h3-19H2,1-2H3 SXTULBAGGXUEQH-UHFFFAOYSA-N 312.53 Propyl heptadecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 111-06-8 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-8-9-10-11-12-13-14-15-16-17-18-20(21)22-19-6-4-2/h3-19H2,1-2H3 GLYJVQDYLFAUFC-UHFFFAOYSA-N 312.53 Butyl hexadecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 71801-23-5 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-8-9-10-11-12-13-14-15-17-19-22-20(21)18-16-6-4-2/h3-19H2,1-2H3 SMMNCBBCUVMKHP-UHFFFAOYSA-N 312.53 Tetradecyl hexanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 20292-09-5 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-9-10-11-12-13-15-17-19-22-20(21)18-16-14-8-6-4-2/h3-19H2,1-2H3 OYQTUTLMOLEYNR-UHFFFAOYSA-N 312.53 Dodecyl octanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 42231-99-2 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-9-10-11-12-13-14-15-16-18-20(21)22-19-17-8-6-4-2/h3-19H2,1-2H3 JIFCVUWJQMDNTN-UHFFFAOYSA-N 312.53 Hexyl tetradecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 5303-24-2 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-9-11-12-13-14-16-18-20(21)22-19-17-15-10-8-6-4-2/h3-19H2,1-2H3 BBZAGOMQOSEWBH-UHFFFAOYSA-N 312.53 Octyl dodecanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. 1654-86-0 2 C20H40O2 InChI=1S/C20H40O2/c1-3-5-7-9-11-13-15-17-19-22-20(21)18-16-14-12-10-8-6-4-2/h3-19H2,1-2H3 XAKXZZPEUKNHMA-UHFFFAOYSA-N 312.53 Decyl decanoate Methyl, ethyl and butyl esters purchased from Applied Science Laboratories; propyl and hexyl esters, formate, acetate, propanoate and butyrate prepared by direct esterification; other esters synthesized by transesterification; purified. Acetonitrile with Esters (C20)