Ari L. Horvath 1 2.5e+01 Ambient temperature 2 2.5 °C -1 7.5e-01 Percent mass fraction (1) 2 7.5 1 -2 8.0e-02 Percent mass fraction (2) 2 8.0 1 1 -3 1.139e-03 Mole fraction - Liquid (1) 4 1.139 1 -3 5.278e-03 Mole fraction - Liquid (2) 4 5.278 1 1 5.61e+01 Ambient temperature 3 5.61 °C -1 8.0e-01 Percent mass fraction (1) 2 8.0 1 -1 1.7e-01 Percent mass fraction (2) 2 1.7 1 2 -3 1.216e-03 Mole fraction - Liquid (1) 4 1.216 1 -2 1.116e-02 Mole fraction - Liquid (2) 4 1.116 1 1 Solubility, Solubility data series A flask was charged with a trichloromethane and water mixture of approximately the desired composition. The system was allowed to equilibrate in a water bath at the desired temperature. Samples were withdrawn from the two layers and concentrations were determined. The analytical techniques are described elsewhere [1]. The International Union of Pure and Applied Chemistry Conti, J. J.; Othmer, D. F. Unpublished data. unpublished Conti, J. J.; Othmer, D. F.; Gilmont, R.; J. Chem. Eng. Data 1960, 5, 301-7. paper https://doi.org/10.1021/je60007a019 67-66-3 1 CHCl3 InChI=1S/CHCl3/c2-1(3)4/h1H HEDRZPFGACZZDS-UHFFFAOYSA-N 119.378 Trichloromethane U. S. P. grade. Washed with $\ce{H2SO4}$ and $\ce{K2CO3}$ solutions and then distilled. Only the center cut was used. 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Deionized, distilled twice before use. Trichloromethane with Water