Ari L. Horvath 1 1.5e+01 Ambient temperature 2 1.5 °C -1 2.0e-01 Percent mass fraction (1) 2 2.0 1 1 -2 1.31e-02 Mole fraction - Liquid (1) 3 1.31 1 -4 1.11e-04 Mole (1) per 100 gram 3 1.11 mol/g 1 Solubility, Solubility data series Weighted mixtures of water and trichloromethane were shaken in sealed tubes in a water bath until the equilibrium had been established. After separation in two layers, a sample of the organic phase was taken and the water content of the mixture was determined by titration with a solution of cobalt chloride in anhydrous acetone. For further details, see [1]. The International Union of Pure and Applied Chemistry Wilson, P. E.; J. Am. Chem. Soc. 1921, 43, 710. paper https://doi.org/10.1021/ja01437a003 De Minjer, C. H.; Ph.D. Dissertation, Technische Hoogeschool, Delft, The Netherlands, 1939, 165 pp. dissertation 67-66-3 1 CHCl3 InChI=1S/CHCl3/c2-1(3)4/h1H HEDRZPFGACZZDS-UHFFFAOYSA-N 119.378 Trichloromethane Distilled. 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Commercial grade, washed with $\ce{H2SO4}$ and $\ce{K2CO3}$ solutions, followed by distillation before use. Trichloromethane with Water