Ari L. Horvath 1 1.5e+01 Ambient temperature 2 1.5 °C 0 5.7e+00 Amount concentration (1) 2 5.7 mol/m3 1 -3 7.13e-03 Percent mass fraction (1) 3 7.13 1 -4 5.47e-04 Mole fraction - Liquid (1) 3 5.47 1 1 2.5e+01 Ambient temperature 2 2.5 °C 0 7.5e+00 Amount concentration (1) 2 7.5 mol/m3 2 -3 9.49e-03 Percent mass fraction (1) 3 9.49 1 -4 7.28e-04 Mole fraction - Liquid (1) 3 7.28 1 1 3.0e+01 Ambient temperature 2 3.0 °C 0 8.4e+00 Amount concentration (1) 2 8.4 mol/m3 3 -2 1.07e-02 Percent mass fraction (1) 3 1.07 1 -4 8.21e-04 Mole fraction - Liquid (1) 3 8.21 1 1 3.5e+01 Ambient temperature 2 3.5 °C 1 1.03e+01 Amount concentration (1) 3 1.03 mol/m3 4 -2 1.32e-02 Percent mass fraction (1) 3 1.32 1 -3 1.013e-03 Mole fraction - Liquid (1) 4 1.013 1 1 Solubility, Solubility data series The saturation of heavy water with tetrachloromethane was done in a closed system, protected from atmospheric moisture, and placed in a constant temperature water bath. The solubility of heavy water in tetrachloromethane was measured using the Karl Fischer titration method with a 'dead stop' end-point determination [1]. 15 Trials were done at each temperature. The International Union of Pure and Applied Chemistry Wernimont, G.; Hopkinson, F. J. Ind. Eng. Chem., Anal. Ed. 1943, 272. paper https://doi.org/10.1021/i560116a017 Glasoe, P. K.; Schultz, S. D.; J. Chem. Eng. Data 1972, 17, 66-8. paper https://doi.org/10.1021/je60052a025 56-23-5 2 CCl4 InChI=1S/CCl4/c2-1(3,4)5 VZGDMQKNWNREIO-UHFFFAOYSA-N 153.823 Tetrachloromethane Source not given. Reagent grade, purified by distillation before use. 7789-20-0 1 D2O InChI=1S/H2O/h1H2/i/hD2 XLYOFNOQVPJJNP-ZSJDYOACSA-N 20.0276 Water-d2 Source not given, 99.8% pure, used as received. Water-d2 with Tetrachloromethane