Ari L. Horvath 1 1.5e+01 Ambient temperature 2 1.5 °C 1 -3 3.96e-03 Percent mass fraction (1) 3 3.96 1 -4 3.38e-04 Mole fraction - Liquid (1) 3 3.38 1 1 2.0e+01 Ambient temperature 2 2.0 °C 2 -3 4.81e-03 Percent mass fraction (1) 3 4.81 1 -4 4.10e-04 Mole fraction - Liquid (1) 3 4.10 1 1 2.5e+01 Ambient temperature 2 2.5 °C 3 -3 5.90e-03 Percent mass fraction (1) 3 5.90 1 -4 5.03e-04 Mole fraction - Liquid (1) 3 5.03 1 1 Solubility, Solubility data series An about 1 to 5 ratio of water/tetrachloromethane mixture was rotated in a thermostat for 12 hours. After the equilibrium was attained, samples were taken and filtered through cottonwool. The determination of the water content was based upon the reaction witha-naphthoxydichlorophosphine. The evolved $\ce{HCl}$ was absorbed in water and titrated with $\ce{NaOH}$ solution [1]. Two to three successive determinations were carried out with the tetrachloromethane. The International Union of Pure and Applied Chemistry Bell, R. P.; J. Chem. Soc. 1932, 2903. paper https://doi.org/10.1039/jr9320002903 Bell, R. P.; J. Chem. Soc. 1932, 2905-11. paper https://doi.org/10.1039/jr9320002905 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Merck reagent, analytical grade, redistilled before use. 56-23-5 1 CCl4 InChI=1S/CCl4/c2-1(3,4)5 VZGDMQKNWNREIO-UHFFFAOYSA-N 153.823 Tetrachloromethane Distilled (compiler). Tetrachloromethane with Water