Ari L. Horvath 1 2.5e+01 Ambient temperature 2 2.5 °C -3 1.017e-03 Mole (1) per 100 gram 4 1.017 mol/g 1 -2 2.04e-02 Percent mass fraction (1) 3 2.04 1 -3 2.721e-03 Mole fraction - Liquid (1) 4 2.721 1 1 Solubility, Solubility data series A 1 to 15 volume ratio mixture of heavy water and diiodomethane was introduced into an equilibration flask and then lowered into a water thermostat bath. The assembly was shaken mechanically for about 90 minutes at constant temperature. The amount of heavy water in the organic phase was determined by a modified Karl Fischer titration method. The determination was done in triplicate. The description was taken from a secondary source [1]. The original report is no longer available. The International Union of Pure and Applied Chemistry Eidinoff, M. L. In "Production of Heavy Water", National Nuclear Energy Series Division III-Vol. 4F, Murphy, G. M.; Urey, H. C.; Kirshenbaum, I.; Eds.; McGraw-Hill: New York, 1955; Part II, Chapter 7, pp 129-44. chapter Hutchinson, C. A.; Lyon, A. M.; Columbia University Report A-745, July 1, 1943. report 75-11-6 2 CH2I2 InChI=1S/CH2I2/c2-1-3/h1H2 NZZFYRREKKOMAT-UHFFFAOYSA-N 267.836 Diiodomethane Source not given, purified and dried before use. 7789-20-0 1 D2O InChI=1S/H2O/h1H2/i/hD2 XLYOFNOQVPJJNP-ZSJDYOACSA-N 20.0276 Water-d2 Source and purity not given. Water-d2 with Diiodomethane