Ari L. Horvath 1 2.50e+01 Ambient temperature 3 2.50 °C 0 3.11e+00 Amount concentration (1) 3 3.11 mol/m3 1 -2 8.35e-02 Percent mass fraction (1) 3 8.35 1 -5 5.62e-05 Mole fraction - Liquid (1) 3 5.62 1 1 Solubility, Solubility data series Water was mixed with diiodomethanme in a glass-stoppered Erlenmeyer flask which was then placed in a constant temperature bath and rotated for 30 hours. The organic halide content of the aqueous solution was extracted with n-hexane. The optical density of the extract was measured against a nhexane blank using a Beckman spectrophotometer [1]. The International Union of Pure and Applied Chemistry Andrews, L. J.; Keefer, R. M.; J. Am. Chem. Soc. 1949, 71, 3644-77. paper https://doi.org/10.1021/ja01179a018 Andrews, L. J.; Keefer, R. M.; J. Am. Chem. Soc. 1951, 73, 5733-6. paper https://doi.org/10.1021/ja01156a072 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Distilled (compiler). 75-11-6 1 CH2I2 InChI=1S/CH2I2/c2-1-3/h1H2 NZZFYRREKKOMAT-UHFFFAOYSA-N 267.836 Diiodomethane Prepared from iodoform at the University of California; BP = 71.0 - 71.5°C at 18 mmHg. Diiodomethane with Water