{"compilation": {"title": "Solubility data from IUPAC SDS Volume 60 (page ?) - Dichloromethane with Water", "publisher": "The International Union of Pure and Applied Chemistry", "keywords": "Solubility, Solubility data series", "compilers": "Ari L. Horvath", "sources": [{"citation": "Donahue, D. J.; Bartell, F. E.; J. Phys. Chem. 1952, 56, 480-4.", "pubtype": "paper", "url": "https://doi.org/10.1021/j150496a016"}], "system": "Dichloromethane with Water", "substances": [{"constituent": 2, "name": "Water", "formula": "H2O", "molweight": 18.0153, "casrn": "7732-18-5", "inchi": "InChI=1S/H2O/h1H2", "inchikey": "XLYOFNOQVPJJNP-UHFFFAOYSA-N", "sample": "Purified by distillation."}, {"constituent": 1, "name": "Dichloromethane", "formula": "CH2Cl2", "molweight": 84.9326, "casrn": "75-09-2", "inchi": "InChI=1S/CH2Cl2/c2-1-3/h1H2", "inchikey": "YMWUJEATGCHHMB-UHFFFAOYSA-N", "sample": "Reagent grade, purified by fractional distillation before use."}], "method": "A mixture of dichloromethane and water was placed in a glass stoppered flask and was shaken intermittently for at least three days in a water bath held at constant temperature. The organic phase was analyzed for water content using the Karl Fischer titration methods. The concentration of dichloromethane in the aqueous phase was analyzed interferometrically.", "dataset": [{"series": 1, "points": [{"pntnum": 1, "conditions": [{"property": "Ambient temperature", "number": "2.5e+01", "significand": "2.5", "exponent": "1", "sigfigs": "2", "unit": "°C"}], "data": [{"property": "Mole fraction - Liquid (1)", "number": "4.2e-03", "significand": "4.2", "exponent": "-3", "sigfigs": "2", "unit": "1"}, {"property": "Mole fraction - Liquid (2)", "number": "1.13e-02", "significand": "1.13", "exponent": "-2", "sigfigs": "3", "unit": "1"}], "supplemental": [{"property": "Percent mass fraction (1)", "number": "1.950e+00", "significand": "1.950", "exponent": "0", "sigfigs": "4", "unit": "1"}, {"property": "Percent mass fraction (2)", "number": "2.42e-01", "significand": "2.42", "exponent": "-1", "sigfigs": "3", "unit": "1"}]}]}]}}