Ari L. Horvath 1 3.0e+01 Ambient temperature 2 3.0 °C -5 6.76e-05 Mass fraction (1) 3 6.76 1 1 -4 9.78e-04 Mole fraction - Liquid (1) 3 9.78 1 -6 3.75e-06 Mole (1) per 100 gram 3 3.75 mol/g 1 5.0e+01 Ambient temperature 2 5.0 °C -4 2.12e-04 Mass fraction (1) 3 2.12 1 2 -3 3.060e-03 Mole fraction - Liquid (1) 4 3.060 1 -5 1.18e-05 Mole (1) per 100 gram 3 1.18 mol/g 1 Solubility, Solubility data series The Alexejew's synthetic method of solubility determination was used [1]. A fixed weight of water and 1,1,2,3,4,4-hexachloro-1,3-butadiene was sealed in a tube and subjected to gradually increasing temperature with constant agitation. The appearance of an opalescence or clouding was an indication of saturation temperature. The temperature was then allowed to fall and an observation made, while the tube was constantly agitated, to establish the temperature of the first appearance of opalescence. The observation was repeated several times. The International Union of Pure and Applied Chemistry Alexejew, W.; Ann. Phys. Chem. 28, 305 (1886). paper https://doi.org/10.1002/andp.18862640611 Simonov, V. D.; Pogulyai, V. E.; Shamsutdinov, T. M.; Russ. J. Phys. Chem. 1970, 44, 1755-7. paper 7732-18-5 2 H2O InChI=1S/H2O/h1H2 XLYOFNOQVPJJNP-UHFFFAOYSA-N 18.0153 Water Synthesized by the authors, further purified by distillation. 87-68-3 1 C4Cl6 InChI=1S/C4Cl6/c5-1(3(7)8)2(6)4(9)10 RWNKSTSCBHKHTB-UHFFFAOYSA-N 260.761 1,1,2,3,4,4-Hexachloro-1,3-butadiene Distilled (compiler). 1,1,2,3,4,4-Hexachloro-1,3-butadiene with Water