{"compilation": {"title": "Solubility data from IUPAC SDS Volume 69 (page ?) - Methanol with Xylene (mix) and Water", "publisher": "The International Union of Pure and Applied Chemistry", "keywords": "Solubility, Solubility data series", "compilers": "Adam Skrzecz", "sources": [{"citation": "Hartley, J.; J. Soc. Chem. Ind. (London) 69, 60-1 (1950).", "pubtype": "paper", "url": "https://doi.org/10.1002/jctb.5000690208"}], "system": "Methanol with Xylene (mix) and Water", "substances": [{"constituent": 1, "name": "Methanol", "formula": "CH4O", "molweight": 32.0419, "casrn": "67-56-1", "inchi": "InChI=1S/CH4O/c1-2/h2H,1H3", "inchikey": "OKKJLVBELUTLKV-UHFFFAOYSA-N", "sample": "BDH, sulpher free; distilled; fraction boiling at the range 140-142°C was used."}, {"constituent": 2, "name": "Xylene (isomer mix)", "formula": "C8H10", "molweight": 0.0, "casrn": "1330-20-7", "sample": "Source not specified; absolute alcohol; used as received."}, {"constituent": 3, "name": "Water", "formula": "H2O", "molweight": 18.0153, "casrn": "7732-18-5", "inchi": "InChI=1S/H2O/h1H2", "inchikey": "XLYOFNOQVPJJNP-UHFFFAOYSA-N", "sample": "Distilled"}], "method": "The titration method was used. Binary mixtures of known volumes were titrated with the third component in glass-stoppered bottles until, after vigorously shaking, the mixture became turbid. The equilibrium phases were determined by titrating with water binary methanol-xylene mixtures. The xylene-rich phase was at the beginning the lower layer, but addition of water caused this phase to separate as the upper layer. To determine tie immersed in a thermostat bath, shaken, and after separation one component of each phase was analyzed by the Karl Fischer reagent and xylene, in the hydrocarbon-rich phase, was determined by extraction with water. The results were presented on a Gibbs triangle together with binodal curve.", "dataset": [{"series": 1, "title": "Compositions along the saturation curve", "points": [{"pntnum": 1, "conditions": [{"property": "Ambient temperature", "number": "2.0e+01", "significand": "2.0", "exponent": "1", "sigfigs": "2", "unit": "°C"}, {"property": "Ambient temperature", "number": "2.932e+02", "significand": "2.932", "exponent": "2", "sigfigs": "4", "unit": "$\\pu{K}$"}], "data": [{"property": "Mole fraction - Liquid (1)", "number": "4.19e-01", "significand": "4.19", "exponent": "-1", "sigfigs": "3", "unit": "1"}, {"property": "Mole fraction - Liquid (2)", "number": "5.53e-01", "significand": "5.53", "exponent": "-1", "sigfigs": "3", "unit": "1"}], "supplemental": [{"property": "Mass fraction (1)", "number": "1.85e-01", "significand": "1.85", "exponent": "-1", "sigfigs": "3", "unit": "1"}, {"property": "Mass fraction (2)", "number": "8.08e-01", "significand": "8.08", "exponent": "-1", "sigfigs": "3", 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