{"compilation": {"title": "Solubility data from IUPAC SDS Volume 69 (page ?) - Ethanol with n-Hexane with Water", "publisher": "The International Union of Pure and Applied Chemistry", "keywords": "Solubility, Solubility data series", "compilers": "Adam Skrzecz", "sources": [{"citation": "Moriyoshi, T.; Uosaki, Y.; Matsuura, H.; Nishimoto, W.; J. Chem. Thermodyn, 20, 551 (1988).", "pubtype": "paper", "url": "https://doi.org/10.1016/0021-9614(88)90083-3"}], "system": "Ethanol with n-Hexane with Water", "substances": [{"constituent": 1, "name": "Ethanol", "formula": "C2H6O", "molweight": 46.0684, "casrn": "64-17-5", "inchi": "InChI=1S/C2H6O/c1-2-3/h3H,2H2,1H3", "inchikey": "LFQSCWFLJHTTHZ-UHFFFAOYSA-N", "sample": "Source not specified; dried by refluxing with $\\ce{CaO}$, followed by the Lund-Bjerrum magnesium method, distilled."}, {"constituent": 2, "name": "Hexane", "formula": "C6H14", "molweight": 86.1754, "casrn": "110-54-3", "inchi": "InChI=1S/C6H14/c1-3-5-6-4-2/h3-6H2,1-2H3", "inchikey": "VLKZOEOYAKHREP-UHFFFAOYSA-N", "sample": "Source not specified; shaken with conc. $\\ce{H2SO4}$, neutralized with aq. $\\ce{NaOH}$, dried over CaC $\\ce{I2}$, distilled."}, {"constituent": 3, "name": "Water", "formula": "H2O", "molweight": 18.0153, "casrn": "7732-18-5", "inchi": "InChI=1S/H2O/h1H2", "inchikey": "XLYOFNOQVPJJNP-UHFFFAOYSA-N", "sample": "De-ionized, distilled over $\\ce{KMnO4}$, redistilled."}], "method": "The experimental apparatus consisted of a high-pressure equilibrium cell, two hand operated pumps, a pressure exchanger, and two pressure gauges. The equilibrium cell, a stainless-steel cylinder of 50 mL capacity, with mechanical stirrer was immersed in a thermostat. The mixture, prepared by mass, were stirred under the desired conditions for at least 8 h and then allowed to settle for 2 h. Samples of each layer were withdrawn for GLC analysis (glass column, 3.2 mm i.d., 150 cm long, packed with PEG-6000 Shimalite F; T/K=343; thermal-conductivity detector equipped with electronic intergrator). Acetone was used as an inert standard. Compositions were determined from the peak-area ratio and the calibration curve. 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